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High-Percentage Success Method for Preparing and Pre-Evaluating Tungsten Tips for Atomic-Resolution Scanning Tunneling Microscopy

机译:用于制备和预评估钨的高百分比成功方法   原子分辨率扫描隧道显微镜技巧

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摘要

A custom double-lamella method is presented for electrochemically etchingtungsten wire for use as tips in scanning tunneling microscopy (STM). Forcomparison, tips were also manufactured in-house using numerous conventionalmethods and examined using an optical microscope. Both sets of tips were usedto obtain STM images of highly-oriented pyrolytic graphite, the quality ofwhich varied. The clarity of the STM images was found to be correlated to theoptically-measured cone angle of the STM tip, with larger cone anglesconsistently producing atomically resolved images. The custom etching proceduredescribed allows one to create larger cone angles and consequently provedsuperior in reliably producing high-quality tips.
机译:提出了一种定制的双层方法,用于电化学蚀刻钨丝,用作扫描隧道显微镜(STM)的尖端。为了进行比较,还使用多种常规方法在内部制造了笔尖,并使用光学显微镜对其进行了检查。两组尖端均用于获得高取向热解石墨的STM图像,其质量各不相同。发现STM图像的清晰度与STM尖端的光学测量锥角相关,其中较大的锥角一致地产生原子分辨图像。所描述的定制蚀刻程序允许创建更大的锥角,因此被证明在可靠地生产高质量笔尖方面具有优势。

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